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Atomic Force Microscopy01:08

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The AFM Probe
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Optimising multi-frame ADF-STEM for high-precision atomic-resolution strain mapping.

Lewys Jones1, Sigurd Wenner2, Magnus Nord2

  • 1Department of Materials, University of Oxford, Oxford, OX13PH, UK.

Ultramicroscopy
|April 23, 2017
PubMed
Summary
This summary is machine-generated.

Optimizing multi-frame acquisition in scanning transmission electron microscopy significantly reduces scanning artifacts. This approach enhances atomic-resolution strain mapping precision, crucial for materials science defect analysis.

Keywords:
ADF-STEMAluminium alloysDensity functional calculationsExperiment designStrain in crystals/solids

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Area of Science:

  • Materials Science
  • Condensed Matter Physics
  • Electron Microscopy

Background:

  • Annular dark-field scanning transmission electron microscopy (ADF-STEM) enables atomic-scale crystal defect studies.
  • Low-frequency scanning distortions in single frames limit accurate atomic-resolution strain mapping.

Purpose of the Study:

  • To determine the optimal number of frames for multi-frame acquisition in ADF-STEM for maximum strain mapping precision.
  • To investigate dose fractionation strategies for improved strain accuracy under a fixed electron budget.

Main Methods:

  • Utilized a non-rigid image registration procedure prior to established strain mapping techniques.
  • Analyzed the impact of varying the number of frames in image series on strain mapping precision.
  • Investigated dose fractionation for a fixed total electron dose.

Main Results:

  • Achieved over 70% reduction in scanning artifacts with image series of 20-30 frames.
  • Strain mapping precision showed little improvement for series longer than 30 frames.
  • Optimized approach validated by studying strain fields around an aluminum alloy precipitate.

Conclusions:

  • Multi-frame acquisition with 20-30 frames offers optimal strain mapping precision in ADF-STEM.
  • The optimized method enhances accuracy for studying strain fields in materials, verified by DFT.
  • This work provides a guideline for maximizing strain accuracy in ADF-STEM imaging.