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Line-rotated remapping for high-resolution electron backscatter diffraction.

Yongzhe Wang1, Nicolas Brodusch2, Raynald Gauvin2

  • 1The State Key Lab of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, 1295 Dingxu Road, Shanghai 200050, China; Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing 100049, China.

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|September 23, 2022
PubMed
Summary
This summary is machine-generated.

A new method called line-rotated remapping (LRR) accurately analyzes electron backscatter diffraction patterns with significant rotations. This technique improves strain measurements in materials science by precisely mapping crystal orientations.

Keywords:
Elastic strainHigh-resolution EBSDLattice rotationLine-rotated remapping

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Area of Science:

  • Materials Science
  • Crystallography
  • Electron Microscopy

Background:

  • Electron Backscatter Diffraction (EBSD) is crucial for analyzing material microstructures.
  • Accurate crystallographic orientation mapping is essential for understanding material properties.
  • Large lattice rotations in EBSD patterns pose challenges for conventional analysis methods.

Purpose of the Study:

  • To introduce a novel method, line-rotated remapping (LRR), for high-resolution EBSD pattern analysis.
  • To address the challenge of remapping EBSD patterns with large rotations.
  • To enhance the accuracy of strain and rotation measurements in materials.

Main Methods:

  • Developed line-rotated remapping (LRR) by modifying cross-correlation displacements based on Kikuchi lines and reference patterns.
  • Determined finite rotation matrices using Kikuchi line parameters to align test patterns with reference patterns.
  • Applied LRR to simulated silicon (Si) patterns and experimental nickel (Ni) single crystal samples.

Main Results:

  • Achieved measurement errors below 1.0 × 10-3 for lattice rotations up to 26° in simulated Si patterns.
  • Demonstrated LRR's capability to quantitatively characterize rotations and elastic strains in a Ni single crystal under mechanical loading.
  • Observed that the maximum remappable angle decreases with specimen-screen distance, impacting matched Kikuchi lines.

Conclusions:

  • Line-rotated remapping (LRR) is a promising technique for improving strain measurements in EBSD, especially with large rotations.
  • LRR offers high accuracy for crystallographic orientation analysis in challenging EBSD datasets.
  • Further experimental validation is needed to fully assess LRR's performance, particularly regarding pattern center and image contrast.