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Updated: Jun 3, 2025

One-pot Microwave-assisted Conversion of Anomeric Nitrate-esters to Trichloroacetimidates
Published on: January 15, 2018
rac-2-{3-[1-(Acet-yloxy)eth-yl]-2,2-di-methyl-cyclobut-yl}acetic acid
Dieter Schollmeyer1, Paul Jirsch1, Heiner Detert1
1University of Mainz, Department of Chemistry, Duesbergweg 10-14, 55099 Mainz, Germany.
Abstract:
The title compound, C12H20O4, was prepared from α-pinene in three steps. The ester and acid moieties are cis on the slightly folded cyclo-butane ring. In the crystal, carb-oxy-lic acid bound dimers form layers parallel to (202).
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